化工社化工社 化学情報印刷レポート · 研究参考用
Thymine → Thymine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Thymine | HCID 1135 | — |
| 反応物 | Tetrabutylammonium Hydroxide | HCID 2723671 | — |
| 溶媒 | Dimethylformamide | HCID 6228 | — |
| 生成物 | Thymine | HCID 1135 | — |
| 生成物 | Tetrabutylammonium | HCID 16028 | — |
反応手順
1.5M Tetra(n-butyl)ammonium hydroxide (4.22 ml., 6.335 mole) was added to a suspension of thymine (0.913 g., 7.24 mole) in dimethylformamide (15 ml. ). The mixture was stirred for 10 minutes, and the dimethylformamide was removed in vacuo. Additional dimethylformamide (20 ml. ) was added to the white residue, and removed in vacuo. This process was repeated four times and the residue was dried under a vacuum (0.1 mm) at 50° C. overnight affording the tetra(n-butyl)ammonium salt of thymine.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05414000 |
| 出典データセット | uspto-grants-1995_05 |
| ORD ID | ord-12b85e5ec8824ed7a2d19a54c001d385 |
| 出典メモ | uspto-grants-1995_05 |