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HRID 36326作成日:2026年10月26日

Thymine → Thymine

https://huagongshe.com/reaction/36326

反応式

関与物質

役割名称HCID仕込み量
反応物ThymineHCID 1135—
反応物Tetrabutylammonium HydroxideHCID 2723671—
溶媒DimethylformamideHCID 6228—
生成物ThymineHCID 1135—
生成物TetrabutylammoniumHCID 16028—

反応手順

1.5M Tetra(n-butyl)ammonium hydroxide (4.22 ml., 6.335 mole) was added to a suspension of thymine (0.913 g., 7.24 mole) in dimethylformamide (15 ml. ). The mixture was stirred for 10 minutes, and the dimethylformamide was removed in vacuo. Additional dimethylformamide (20 ml. ) was added to the white residue, and removed in vacuo. This process was repeated four times and the residue was dried under a vacuum (0.1 mm) at 50° C. overnight affording the tetra(n-butyl)ammonium salt of thymine.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US05414000
出典データセットuspto-grants-1995_05
ORD IDord-12b85e5ec8824ed7a2d19a54c001d385
出典メモuspto-grants-1995_05