化工社化工社 化学情報印刷レポート · 研究参考用
Ethyl Acetate → Benzenebutanal, 4-(phenylmethoxy)-
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ethyl Acetate | HCID 8857 | — |
| 反応物 | Sulfuric acid magnesium salt (1:1) | HCID 24083 | — |
| 反応物 | Norepinephrine | HCID 439260 | — |
| 触媒 | Platinum | HCID 23939 | — |
| 生成物 | Benzenebutanal, 4-(phenylmethoxy)- | HCID 11086308 | — |
反応手順
A solution of 4-(4-benzyloxyphenyl)-butanal (52.4 g, 206 mmol) in 150 mL ethyl acetate (1.4M solution) was prepared and set aside. 10% platinum on carbon (3.40 g) was prewetted with ethyl acetate and transferred to the reactor. To this was added magnesium sulfate (60.0 g, 500 mmol), followed by the ethyl acetate solution of (trimethylsilyl)-protected norepinephrine prepared as described in Example 1.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05874601 |
| 出典データセット | uspto-grants-1999_02 |
| ORD ID | ord-becb9cf850d841398405eae6e1336a80 |
| 出典メモ | uspto-grants-1999_02 |