化工社化工社 化学情報印刷レポート · 研究参考用
Mercaptoethanesulfonic acid → 2-Nitro-5-sulphoethylthio-paraphenylenediamine monohydrate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Mercaptoethanesulfonic acid | HCID 598 | — |
| 反応物 | Sodium | HCID 5360545 | — |
| 反応物 | 1,4-Benzenediamine, 2-chloro-5-nitro- | HCID 5484290 | — |
| 生成物 | 2-Nitro-5-sulphoethylthio-paraphenylenediamine monohydrate | HCID 131721132 | — |
反応手順
18.7 g (0.1 mol) of 2-nitro-5-chloropara-phenylenediamine and 24.6 g (0.15 mol) of the sodium salt of 2-mercaptoethanesulphonic acid were used as the starting materials to give yellow-orange crystals (27.6 g) melting above 260° C., whose elemental analysis calculated for C8H11N3O5S2.H2O was:
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05874618 |
| 出典データセット | uspto-grants-1999_02 |
| ORD ID | ord-316bb4386f61461f8edfab49172886a8 |
| 出典メモ | uspto-grants-1999_02 |