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HRID 363825作成日:2026年10月26日

Water → Phenol

https://huagongshe.com/reaction/363825

反応式

関与物質

役割名称HCID仕込み量
反応物WaterHCID 962—
反応物PhenolHCID 996—
反応物Bisphenol AHCID 6623—
溶媒AcetoneHCID 180—
生成物PhenolHCID 996—
生成物2-Hydroxy-alpha-methylstyreneHCID 11297992—

反応手順

The mother liquor from the primary system contains water, acetone, impurities and residual BPA. This mother liquor is passed through preheaters into a flash chamber where the water, acetone and a portion of the phenol is flashed to a vapor. This vapor is fed to a distillation column for separating the water and acetone from the lower vapor pressure phenol. The bottoms stream from the flash chamber includes a concentration of impurities and residual BPA in a phenol carrier. From this stream, a small purge is taken to a catalytic decomposition zone where the phenol is distilled overhead and the BPA and impurities are cleaved at high temperature to form phenol and isopropenyl phenol. Phenol is recovered as raw material and recycled to the reaction zone. Uncleavable "heavies" and polymers are purged from the system as "tars." The balance of the flash pot bottoms stream is recycled to the reaction zone.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US05874644
出典データセットuspto-grants-1999_02
ORD IDord-5116378800f44fad8f253843eeb6a29f
出典メモuspto-grants-1999_02