化工社化工社 化学情報印刷レポート · 研究参考用
Isobutyraldehyde → isobutyraldehyde AEEA
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Isobutyraldehyde | HCID 6561 | — |
| 反応物 | 2-Hydroxyputrescine | HCID 164656 | — |
| 生成物 | isobutyraldehyde AEEA | HCID 131718993 | — |
反応手順
In a typical experiment, isobutyraldehyde and aminoethylethanolamine (AEEA) were pumped separately from weighed feed tanks using adjustable metering pumps. Isobutyraldehyde was pumped at a rate of 0.29 lb/hr and AEEA at a rate of 0.37 lb/hr, giving an isobutyraldehyde/AEEA feed mole ratio of approximately 1.10/1 and a liquid hourly space velocity of 0.5 g total liquid feed/hr/ml catalyst. The two liquid feeds were brought together and allowed to react in a 6-foot coil of 1/4-inch tubing before entering the main reactor. Maximum temperature in this coil of tubing was 64° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05414087 |
| 出典データセット | uspto-grants-1995_05 |
| ORD ID | ord-7272e15fad8f4ddf9923bfd3f29c70c0 |
| 出典メモ | uspto-grants-1995_05 |