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Hydrochloric Acid → Phenylmaleic anhydride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydrochloric Acid | HCID 313 | — |
| 反応物 | Aniline | HCID 6115 | — |
| 反応物 | Maleic Anhydride | HCID 7923 | — |
| 溶媒 | Acetonitrile | HCID 6342 | — |
| 生成物 | Phenylmaleic anhydride | HCID 99174 | 29.2% |
反応手順
Following the general procedure of Example I, 150 mmols of maleic anhydride were reacted with 25 mmols of distilled aniline in 60 mL of acetonitrile and in the presence of 38 mmols of concentrated HCl and 2.5 mmols of cuprous oxide. The process resulted in a 29.2% yield of 3-phenylmaleic anhydride.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04604243 |
| 出典データセット | uspto-grants-1986_08 |
| ORD ID | ord-af992a265b0f4d518bc1668be33d9b29 |
| 出典メモ | uspto-grants-1986_08 |