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HRID 36404作成日:2026年10月23日

Thymine → Thymine

https://huagongshe.com/ja/reaction/36404

反応式

関与物質

役割名称HCID仕込み量
反応物ThymineHCID 1135—
反応物Tetrabutylammonium HydroxideHCID 2723671—
溶媒DimethylformamideHCID 6228—
生成物ThymineHCID 1135—
生成物TetrabutylammoniumHCID 16028—

反応手順

1.5M Tetra(n-butyl)ammonium hydroxide (4.22 ml., 6.335 mmole) was added to a suspension of thymine (0.913 g., 7.24 mmole) in dimethylformamide (15 ml.). The mixture was stirred for 10 minutes, and the dimethylformamide was removed in vacuo. Additional dimethylformamide (20 ml.) was added to the white residue, and removed in vacuo. This process was repeated four times and the residue was dried under a vacuum (0.1 mm) at 50° C. overnight affording the tetra (n-butyl) ammonium salt of thymine.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US05414096
出典データセットuspto-grants-1995_05
ORD IDord-9563b5c96ba04b2ba694ef5e71cd858a
出典メモuspto-grants-1995_05