化工社化工社 化学情報印刷レポート · 研究参考用
Thymine → Thymine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Thymine | HCID 1135 | — |
| 反応物 | Tetrabutylammonium Hydroxide | HCID 2723671 | — |
| 溶媒 | Dimethylformamide | HCID 6228 | — |
| 生成物 | Thymine | HCID 1135 | — |
| 生成物 | Tetrabutylammonium | HCID 16028 | — |
反応手順
1.5M Tetra(n-butyl)ammonium hydroxide (4.22 ml., 6.335 mmole) was added to a suspension of thymine (0.913 g., 7.24 mmole) in dimethylformamide (15 ml.). The mixture was stirred for 10 minutes, and the dimethylformamide was removed in vacuo. Additional dimethylformamide (20 ml.) was added to the white residue, and removed in vacuo. This process was repeated four times and the residue was dried under a vacuum (0.1 mm) at 50° C. overnight affording the tetra (n-butyl) ammonium salt of thymine.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05414096 |
| 出典データセット | uspto-grants-1995_05 |
| ORD ID | ord-9563b5c96ba04b2ba694ef5e71cd858a |
| 出典メモ | uspto-grants-1995_05 |