化工社化工社 化学情報印刷レポート · 研究参考用
Formic Acid → 3-(3,4-Dimethoxyphenyl)propionic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Formic Acid | HCID 284 | — |
| 反応物 | Veratraldehyde | HCID 8419 | — |
| 反応物 | 2,2-Dimethyl-1,3-dioxane-4,6-dione | HCID 16249 | — |
| 溶媒 | Triethylamine | HCID 8471 | — |
| 生成物 | 3-(3,4-Dimethoxyphenyl)propionic acid | HCID 75019 | — |
反応手順
7.2 g (0.05 mol) of Meldrum's acid and 8.3 g (0.05 mol) of veratraldehyde were weighed to 40 ml of the mixture of formic acid and triethylamine recovered by distillation in Example 3. The reaction was carried out and the final product was separated as described in Example 3. The volume of the mixture of formic acid and triethylamine recovered amounted to 28 ml.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05414108 |
| 出典データセット | uspto-grants-1995_05 |
| ORD ID | ord-898655059bc74a8987c73528375cf1ae |
| 出典メモ | uspto-grants-1995_05 |