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Formic Acid → 3-(3,4-Dimethoxyphenyl)propionic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Formic Acid | HCID 284 | — |
| 反応物 | 5-(3,4-Dimethoxybenzylidene)-2,2-dimethyl-1,3-dioxane-4,6-dione | HCID 370314 | — |
| 溶媒 | Triethylamine | HCID 8471 | — |
| 生成物 | 3-(3,4-Dimethoxyphenyl)propionic acid | HCID 75019 | — |
反応手順
After weighing 14.6 g (0.05 mol) of 5-(3,4-dimethoxyphenylmethylene)-2,2-dimethyl-1,3-dioxane-4,6-dione (m.p.: 173° C.) to 50 ml of the mixture of formic acid and triethylamine prepared according to Example 1, the procedure described in Example 1 was followed.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05414108 |
| 出典データセット | uspto-grants-1995_05 |
| ORD ID | ord-6e6c0d15e22f49729264b41a77e38132 |
| 出典メモ | uspto-grants-1995_05 |