化工社化工社 化学情報印刷レポート · 研究参考用
Formic Acid → 3-(3,4-Dimethoxyphenyl)propionic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Formic Acid | HCID 284 | — |
| 反応物 | Veratraldehyde | HCID 8419 | — |
| 反応物 | 2-Phenyl-1,3-dioxane-4,6-dione | HCID 933829 | — |
| 溶媒 | Triethylamine | HCID 8471 | — |
| 生成物 | 3-(3,4-Dimethoxyphenyl)propionic acid | HCID 75019 | — |
反応手順
25 ml of the mixture of formic acid and triethylamine prepared as described in Example 1 were added to a mixture of 4.8 g (0.025 mol) of 2-phenyl-1,3-dioxane-4,6-dione (m.p.: 148° C.) and 4.15 g (0.025 mol) of veratraldehyde. The reaction was carried out according to Example 1.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05414108 |
| 出典データセット | uspto-grants-1995_05 |
| ORD ID | ord-c417891da0c84778979b5f07d0034772 |
| 出典メモ | uspto-grants-1995_05 |