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Oxygen → Allyl methacrylate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Oxygen | HCID 977 | — |
| 反応物 | Azobisisobutyronitrile | HCID 6547 | — |
| 反応物 | N-vinyl-2-pyrrolidone | HCID 6917 | — |
| 反応物 | Lauryl Methacrylate | HCID 8906 | — |
| 反応物 | HCID 178435178 | HCID 178435178 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | Allyl methacrylate | HCID 7274 | — |
反応手順
The dimer of allyl methacrylate, which was prepared according to Example 1, was added in the amount of 3 wt.-% (related to the entire mixture) to the mixture containing 80 wt.-% N-vinylpyrrolidone and 20 wt. % dodecyl methacrylate. The mixture was homogenized, freed of air oxygen and polymerized in the presence of 0.4 wt.-% azobisisobutyronitrile in a polypropylene mold at 60° C. for 16 h. The resulting gel contained, after swelling with water, 72 wt.-% water at G=0.027 MPa. The soluble portion was 2%.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04604440 |
| 出典データセット | uspto-grants-1986_08 |
| ORD ID | ord-63dfbe37c5c74c36ad06ad62153dfd64 |
| 出典メモ | uspto-grants-1986_08 |