化工社化工社 化学情報印刷レポート · 研究参考用
Azobisisobutyronitrile → Allyl methacrylate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Azobisisobutyronitrile | HCID 6547 | — |
| 反応物 | N-vinyl-2-pyrrolidone | HCID 6917 | — |
| 反応物 | Lauryl Methacrylate | HCID 8906 | — |
| 反応物 | HCID 178435178 | HCID 178435178 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | Allyl methacrylate | HCID 7274 | — |
反応手順
The dimer of allyl methacrylate, which was prepared according to Example 1, was added in the amount of 3 wt.-% (based on to the entire mixture) to the mixture containing 90 wt.-% N-vinylpyrrolidone and 10 wt.-% dodecyl methacrylate. The mixture was polymerized in a polypropylene mold at 60° C. for 16 h in the presence of 0.4 wt.-% azobisisobutyronitrile. The resulting gel contained, after swelling with water, 76 wt.-% water at G=0.048 MPa. The soluble extractable portion was 2%.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04604440 |
| 出典データセット | uspto-grants-1986_08 |
| ORD ID | ord-0c898061a2e84a4b86bc75b954ef6864 |
| 出典メモ | uspto-grants-1986_08 |