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HRID 364156作成日:2026年10月27日

Azobisisobutyronitrile → Allyl methacrylate

https://huagongshe.com/reaction/364156

反応式

関与物質

役割名称HCID仕込み量
反応物AzobisisobutyronitrileHCID 6547—
反応物N-vinyl-2-pyrrolidoneHCID 6917—
反応物Lauryl MethacrylateHCID 8906—
反応物HCID 178435178HCID 178435178—
溶媒WaterHCID 962—
生成物Allyl methacrylateHCID 7274—

反応手順

The dimer of allyl methacrylate, which was prepared according to Example 1, was added in the amount of 3 wt.-% (based on to the entire mixture) to the mixture containing 90 wt.-% N-vinylpyrrolidone and 10 wt.-% dodecyl methacrylate. The mixture was polymerized in a polypropylene mold at 60° C. for 16 h in the presence of 0.4 wt.-% azobisisobutyronitrile. The resulting gel contained, after swelling with water, 76 wt.-% water at G=0.048 MPa. The soluble extractable portion was 2%.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US04604440
出典データセットuspto-grants-1986_08
ORD IDord-0c898061a2e84a4b86bc75b954ef6864
出典メモuspto-grants-1986_08