化工社化工社 化学情報印刷レポート · 研究参考用
Azobisisobutyronitrile → Allyl methacrylate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Azobisisobutyronitrile | HCID 6547 | — |
| 反応物 | N-vinyl-2-pyrrolidone | HCID 6917 | — |
| 反応物 | tert-Butyl methacrylate | HCID 11448 | — |
| 反応物 | HCID 178435178 | HCID 178435178 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | Allyl methacrylate | HCID 7274 | — |
反応手順
The dimer of allyl methacrylate, which was prepared according to Example 1, was added to the mixture containing 80 wt.-% N-vinylpyrrolidone and 20 wt.-% tert-butyl methacrylate in the amount of 1 wt.-% on the whole mixture. The mixture was polymerized in a polypropylene mold at 60° C. for 16 h in the presence of 0.4 wt.-% azobisisobutyronitrile. The resulting gel contained, after swelling with water, 67 wt.-% water at G=0.529 MPa.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04604440 |
| 出典データセット | uspto-grants-1986_08 |
| ORD ID | ord-315fd0e0fe13428fa1ac09c97485c2f1 |
| 出典メモ | uspto-grants-1986_08 |