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HRID 364159作成日:2026年10月26日

Azobisisobutyronitrile → Allyl methacrylate

https://huagongshe.com/reaction/364159

反応式

関与物質

役割名称HCID仕込み量
反応物AzobisisobutyronitrileHCID 6547—
反応物N-vinyl-2-pyrrolidoneHCID 6917—
反応物tert-Butyl methacrylateHCID 11448—
反応物HCID 178435178HCID 178435178—
溶媒WaterHCID 962—
生成物Allyl methacrylateHCID 7274—

反応手順

The dimer of allyl methacrylate, which was prepared according to Example 1, was added to the mixture containing 80 wt.-% N-vinylpyrrolidone and 20 wt.-% tert-butyl methacrylate in the amount of 1 wt.-% on the whole mixture. The mixture was polymerized in a polypropylene mold at 60° C. for 16 h in the presence of 0.4 wt.-% azobisisobutyronitrile. The resulting gel contained, after swelling with water, 67 wt.-% water at G=0.529 MPa.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US04604440
出典データセットuspto-grants-1986_08
ORD IDord-315fd0e0fe13428fa1ac09c97485c2f1
出典メモuspto-grants-1986_08