関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Formic Acid | HCID 284 | — |
| 反応物 | 4-Nitrobenzaldehyde | HCID 541 | — |
| 反応物 | 2,2-Dimethyl-1,3-dioxane-4,6-dione | HCID 16249 | — |
| 溶媒 | Triethylamine | HCID 8471 | — |
| 生成物 | 3-(4-Nitrophenyl)propanoic acid | HCID 85526 | — |
反応手順
3.60 g (0.025 mol) of Meldrum's acid and 3.8 g (0.025 mol) of p-nitrobenzaldehyde were weighed in to 25 ml of the mixture of formic acid and triethylamine prepared as described in Example l. The reaction mixture was heated to 105° C. during 1 hour and reacted at the same temperature for 1 hour. The product was isolated according to Example 1.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US05414108 |
|---|
| 出典データセット | uspto-grants-1995_05 |
|---|
| ORD ID | ord-34d196c1fab248819f8d6892c2587e9f |
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| 出典メモ | uspto-grants-1995_05 |
|---|
