Dimethylamine → 2-[2-(Dimethylamino)ethyl]-2,3-dihydro-4,10-dimethyl-1,4-oxazepino[6,7-h]quinoline-5(4H)-thione hydrochloride

反応式

[Cl:1][CH2:2][CH2:3][CH:4]1[CH2:19][N:18]([CH3:20])[C:17](=[S:21])[C:7]2[CH:8]=[CH:9][C:10]3[CH:11]=[CH:12][C:13]([CH3:16])=[N:14][C:15]=3[C:6]=2[O:5]1.[CH3:22][NH:23][CH3:24]>>[ClH:1].[CH3:22][N:23]([CH3:24])[CH2:2][CH2:3][CH:4]1[CH2:19][N:18]([CH3:20])[C:17](=[S:21])[C:7]2[CH:8]=[CH:9][C:10]3[CH:11]=[CH:12][C:13]([CH3:16])=[N:14][C:15]=3[C:6]=2[O:5]1

参加物

反応物 2

HCID 674Dimethylamine

HCID 212715292-(2-chloroethyl)-2,3-dihydro-4,10-dimethyl-1,4-oxazepino[6,7-h)quinoline-5(4H)-thione

生成物 1

HCID 212714572-[2-(Dimethylamino)ethyl]-2,3-dihydro-4,10-dimethyl-1,4-oxazepino[6,7-h]quinoline-5(4H)-thione hydrochloride

実験手順

Following the procedure of Example 31, 2-(2-chloroethyl)-2,3-dihydro-4,10-dimethyl-1,4-oxazepino[6,7-h]quinoline-5(4H)-thione is reacted with dimethylamine to give the title compound.

出典と根拠

ORDレコード: ord-15de92998362459292143ec5364247ab
出典データセット: uspto-grants-1986_08
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US04604388

反応ノート

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