Potassium Carbonate → HCID 178472279、化合物
反応式
[CH2:1]([O:3][CH:4]([PH:8](=[O:12])OCC)[O:5][CH2:6][CH3:7])[CH3:2].[CH:13]1([Mg]Cl)[CH2:18][CH2:17][CH2:16][CH2:15][CH2:14]1.C(=O)([O-])[O-].[K+].[K+]>C(OCC)C.O>[CH:13]1([PH:8](=[O:12])[CH:4]([O:3][CH2:1][CH3:2])[O:5][CH2:6][CH3:7])[CH2:18][CH2:17][CH2:16][CH2:15][CH2:14]1参加物
6
実験手順
Following a procedure analogous to that of Example 1, but using 9.81 g of ethyl diethoxymethylphosphinate and 50 ml of a 2 molar solution of cyclohexylmagnesium chloride in diethyl ether and adding 20.7 g of potassium carbonate in 25 ml of water to precipitate inorganic salts, cyclohexyl(diethoxymethyl)phosphine oxide is obtained as colourless oil.
後処理
- customto precipitate inorganic salts
出典と根拠
- ORDレコード
- ord-c3a82320d5ab433b9198f9b8395980f1
- 出典データセット
- uspto-grants-1995_05
- 特許番号
- US05414133
反応ノート
読み込み中…