Hydrochloric Acid → Benzenediazonium, 4-methoxy-, chloride
反応式
[N:1]([O-])=O.[Na+].[CH3:5][O:6][C:7]1[CH:12]=[CH:11][C:10]([NH2:13])=[CH:9][CH:8]=1.[ClH:14]>O>[Cl-:14].[CH3:5][O:6][C:7]1[CH:12]=[CH:11][C:10]([N+:13]#[N:1])=[CH:9][CH:8]=1参加物
5
実験手順
A solution of 4-methoxy-phenyl-diazonium chloride was prepared by adding dropwise at 0° C. a solution of 1.8 g of sodium nitrite dissolved in 2.5 ml of water to a solution of 3.075 g of p-anisidine dissolved in 25 ml of water and 8.1 ml of concentrated hydrochloric acid. The reaction mixture was allowed to stand for 2 hours.
出典と根拠
- ORDレコード
- ord-d6d25bce37ec4c349c5656b92c48d3e4
- 出典データセット
- uspto-grants-1986_08
- 特許番号
- US04605697
反応ノート
読み込み中…