化工社化工社 化学情報印刷レポート · 研究参考用
Beta-Pinene → (-) Sodium(4S)-p-menth-1-ene-7-sulfonate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Beta-Pinene | HCID 14896 | — |
| 反応物 | Sodium Bisulfite | HCID 23665763 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | (-) Sodium(4S)-p-menth-1-ene-7-sulfonate | HCID 23696841 | — |
反応手順
In a 1 liter, 3-neck flask, 70 grams (0.51 mole) β-pinene and 325 ml water was heated to reflux. Sodium bisulfite, 70 grams, was added at the rate of 13 grams per hour. The solution was refluxed for 7 hours and allowed to stand overnight.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04606851 |
| 出典データセット | uspto-grants-1986_08 |
| ORD ID | ord-535105d41c2445fc90e9acb96f5d350a |
| 出典メモ | uspto-grants-1986_08 |