Aluminum Sulfate → Tris(N-(1-oxotetradecyl)-L-glutamato(2-))dialuminium

HRID 364874

反応式

HRID 364874 の反応式
[C:1]([NH:16][C@H:17]([C:23]([O-:25])=[O:24])[CH2:18][CH2:19][C:20]([O-:22])=[O:21])(=[O:15])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH3:14].[Na+].[Na+].S([O-])([O-])(=O)=O.[Al+3:33].S([O-])([O-])(=O)=O.S([O-])([O-])(=O)=O.[Al+3]>O>[C:1]([NH:16][C@H:17]([C:23]([O-:25])=[O:24])[CH2:18][CH2:19][C:20]([O-:22])=[O:21])(=[O:15])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH3:14].[Al+3:33].[C:1]([NH:16][C@H:17]([C:23]([O-:25])=[O:24])[CH2:18][CH2:19][C:20]([O-:22])=[O:21])(=[O:15])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH3:14].[C:1]([NH:16][C@H:17]([C:23]([O-:25])=[O:24])[CH2:18][CH2:19][C:20]([O-:22])=[O:21])(=[O:15])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH3:14].[Al+3:33]

参加物

4

反応物 2

HCID 24850Aluminum SulfateHCID 71587140Disodium myristoyl glutamate

生成物 1

HCID 56843224Tris(N-(1-oxotetradecyl)-L-glutamato(2-))dialuminium

試薬・触媒・溶媒 1

HCID 962Water溶媒

実験手順

Sodium N-myristoyl-L-glutamate was added to a suspension in which 30 g of sericite had been suspended in 4 liters of water. Then, stirring was fully carried out. Into this suspension was added 60 ml of a 20% aqueous solution of aluminum sulfate in 10 minutes. Then, further stirring was carried out for 10 minutes. Thereafter, the suspension was dehydrated by means of a basket type centrifuge. Then, drying was carried out at 110° C. in a hot-air drying apparatus to produce about 1 kg of a dried product. The dried product thus obtained was crushed by means of a high-speed mixer (hexyl mixer) to a light degree.

後処理

  1. stirringThen, further stirring
  2. customThen, drying
  3. customwas carried out at 110° C. in a hot-air drying apparatus

出典と根拠

ORDレコード
ord-e1103b5d5638410bade466667e08a029
出典データセット
uspto-grants-1986_08
特許番号
US04606914

関連ノート

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