化工社化工社 化学情報印刷レポート · 研究参考用
Benzaldehyde → Ethyl 2-Propyl-3-hydroxy-3-phenylpropionate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Benzaldehyde | HCID 240 | — |
| 反応物 | Ethyl valerate | HCID 10882 | — |
| 生成物 | Ethyl 2-Propyl-3-hydroxy-3-phenylpropionate | HCID 13594173 | — |
反応手順
A 100 milligram sample of the prepared hydroxy-ester is pyrolyzed in a sealed tube at 240°-245° C. for 1 hour. Examination of the pyrolyzate by liquid chromatography indicates that it consists of 60% of unreacted hydroxy-ester and 40% of a 1:1 mixture of ethyl valerate and benzaldehyde.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04607118 |
| 出典データセット | uspto-grants-1986_08 |
| ORD ID | ord-8b090244aaec4db29cb694953bdf1778 |
| 出典メモ | uspto-grants-1986_08 |