関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | N-Methyloctadecylamine | HCID 75539 | — |
| 反応物 | Propanoic acid, 3-(diphenylphosphino)-, ethyl ester | HCID 280676 | — |
| 反応物 | Sodium Methoxide | HCID 10942334 | — |
| 生成物 | 3-(Diphenylphosphanyl)-N-methyl-N-octadecylpropanamide | HCID 53933128 | — |
反応手順
A mixture of 5.7 g ethyl-3-diphenylphosphinopropionate (9.9 mmoles), 5.1 g N-methyl-n-octadecylamine (18.0 mmoles), and 0.3 g sodium methoxide (5.6 mmoles) were first deoxygenated and then heated to 100° C. under a nitrogen atmosphere for 24 hours. The mixture was then cooled and extracted with pentane. The pentane soluble was rotovapped to an oil.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US04608444 |
|---|
| 出典データセット | uspto-grants-1986_08 |
|---|
| ORD ID | ord-742f13ee5dcc41a9afa0a9d6004cf557 |
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| 出典メモ | uspto-grants-1986_08 |
|---|
