関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Hydrogen Peroxide | HCID 784 | — |
| 反応物 | Ethylenediaminetetraacetic Acid | HCID 6049 | — |
| 反応物 | Butyl imino dipropionic acid | HCID 131718997 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | HCID 178444799 | HCID 178444799 | — |
反応手順
100 g butyl imino dipropionic acid (0.46 mol) from example 7a was dissolved in 100 g H2O, whereupon 0.10 g EDTA was added and the temperature was increased to 50° C. After 30 minutes 3.2 g (0.475 mol) 50% hydrogen peroxide was added by drops during 20 minutes and the mixture reacted for 2 hours at 75° C. under a reflux cooler. Then the water was evaporated at 40° C. until a slightly yellow-brown oil formed.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US05415668 |
|---|
| 出典データセット | uspto-grants-1995_05 |
|---|
| ORD ID | ord-21e0230d66d34335bfad3ff73829e671 |
|---|
| 出典メモ | uspto-grants-1995_05 |
|---|
