化工社化工社 化学情報印刷レポート · 研究参考用
Thionyl Chloride → 3-(2-Thienyl)acryloylchloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Thionyl Chloride | HCID 24386 | — |
| 反応物 | 3-Thiophen-2-ylprop-2-enoic acid | HCID 92868 | — |
| 溶媒 | Benzene | HCID 241 | — |
| 生成物 | 3-(2-Thienyl)acryloylchloride | HCID 53411288 | — |
反応手順
65 ml of benzene was added to 10 grams of 3-(2-thienyl)acrylic acid. 7.8 ml of thionyl chloride was added dropwise slowly thereto at ambient temperature. The temperature was elevated to 70° C. and the heating was continued until foaming ceased. Benzene and thionyl chloride were distilled off and the residue was dried thoroughly under reduced pressure.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05415780 |
| 出典データセット | uspto-grants-1995_05 |
| ORD ID | ord-13187ea360704606860b8bea6a1572de |
| 出典メモ | uspto-grants-1995_05 |