化工社化工社 化学情報印刷レポート · 研究参考用
Water → (2,6-Dimethyl-3-nitrophenyl)methanol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Water | HCID 962 | — |
| 反応物 | Sodium Hydroxide | HCID 14798 | — |
| 反応物 | (2,6-Dimethyl-3-nitrophenyl)methyl acetate | HCID 10537042 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 生成物 | (2,6-Dimethyl-3-nitrophenyl)methanol | HCID 10487641 | 82.4% |
反応手順
To a solution of 2,6-dimethyl-3-nitrobenzyl acetate (26.9 g) in methanol (266 ml) was added aqueous 1N sodium hydroxide solution (133 ml) at ambient temperature for 30 minutes. To the mixture was added water, and the precipitate was collected by filtration to give 2,6-dimethyl-3-nitrobenzyl alcohol (18.0 g) as pale yellow crystals.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06127389 |
| 出典データセット | uspto-grants-2000_10 |
| ORD ID | ord-f1fb1725b3bb469d9f57f73a62124038 |
| 出典メモ | uspto-grants-2000_10 |