化工社化工社 化学情報印刷レポート · 研究参考用
Geraniol → 4-Acryloyl-2-geranyloxy-2,3,4,5-tetrahydro-1,4-benzothiazepine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Geraniol | HCID 637566 | — |
| 反応物 | 4-Acryloyl-2-chloro-2,3,4,5-tetrahydro-1,4-benzothiazepine | HCID 15291658 | — |
| 触媒 | Zincchloride | HCID 3007855 | — |
| 生成物 | 4-Acryloyl-2-geranyloxy-2,3,4,5-tetrahydro-1,4-benzothiazepine | HCID 15291652 | 68.3% |
反応手順
The above-mentioned 4-acryloyl-2-chloro-2,3,4,5-tetrahydro-1,4-benzothiazepine (1.0 g), geraniol (0.9 g) and zinc chloride (0.8 g) were reacted in the same manner as in Experimental Example 9 to give 4-acryloyl-2-geranyloxy-2,3,4,5-tetrahydro-1,4-benzothiazepine (1.0 g).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05416066 |
| 出典データセット | uspto-grants-1995_05 |
| ORD ID | ord-d9b3e31b5faf42ceb8283b36db1ef77b |
| 出典メモ | uspto-grants-1995_05 |