1,3,5-Trichlorobenzene → 1,3,5-Trifluorobenzene

HRID 365965

反応式

HRID 365965 の反応式
[F:1][C:2]1[CH:3]=[C:4]([CH:6]=[C:7]([F:9])[CH:8]=1)N.ClC1C=C(Cl)C=C(Cl)C=1.[F-:19]>>[F:1][C:2]1[CH:3]=[C:4]([F:19])[CH:6]=[C:7]([F:9])[CH:8]=1

参加物

4

実験手順

In a further embodiment, the present invention relates to a method for the two step preparation of 3,5-difluoroaniline from 1,3,5-trichlorobenzene. First, an amount of 1,3,5-trichlorobenzene is reacted with a fluoride-containing compound to obtain 1,3,5-trifluorobenzene. Second, the 1,3,5-trifluorobenzene is reacted with aqueous ammonia and a metal oxide or metal hydroxide to obtain the product 3,5-difluoroaniline.

後処理

  1. additioncontaining compound

出典と根拠

ORDレコード
ord-45e0cbdb38d34daab543f555c607bb71
出典データセット
uspto-grants-2000_10
特許番号
US06127577

関連ノート

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