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HRID 366427作成日：2026年10月27日

1-(10,11-Dihydro-5H-dibenzo[a,d]cyclohepten-5-yl)piperazine → cis-7-{4-[4-(10,11-Dihydro-5H-dibenzo[a,d]cyclohepten-5-yl)-piperazin-1-yl]-but-2-envioxy}-2-methyl-benzothiazole

https://huagongshe.com/reaction/366427

反応式

関与物質

役割名称HCID仕込み量
反応物1-(10,11-Dihydro-5H-dibenzo[a,d]cyclohepten-5-yl)piperazineHCID 2735936—
反応物1,4-Dichloro-cis-2-buteneHCID 6432115—
反応物cis-7-(3-Chloroallyloxy)-2-methyl-benzothiazoleHCID 86755936—
生成物cis-7-{4-[4-(10,11-Dihydro-5H-dibenzo[a,d]cyclohepten-5-yl)-piperazin-1-yl]-but-2-envioxy}-2-methyl-benzothiazoleHCID 67851631—
生成物cis-7-(3-Chloroallyloxy)-2-methyl-benzothiazoleHCID 86755936—

反応手順

The title compound was prepared according to Method GA from cis-7-(3-chloroallyloxy)-2-methyl-benzothiazole and 1-(10,11-dihydro-5H-dibenzo[a,d]cyclohepten-5-yl)piperazine. mp 114° C.; LSIMS m/z 496. The cis-7-(3-chloro-allyloxy)-2-methyl-benzothiazole was prepared by Method IV, with cis-1,4-dichloro-2-butene as the alkylating agent.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US06130217
出典データセットuspto-grants-2000_10
ORD IDord-e00a9f5c77f841b29a420b447aaf9417
出典メモuspto-grants-2000_10