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HRID 366428作成日：2026年10月26日

1,4-Dichloro-2-butene, (2E)- → trans-7-{4-[4-(10,11-Dihydro-5H-dibenzo[a,d]cyclohepten-5-yl)-piperazin-1-yl]-but-2-enyloxy}-2-methyl-benzothiazole

https://huagongshe.com/reaction/366428

反応式

関与物質

役割名称HCID仕込み量
反応物1,4-Dichloro-2-butene, (2E)-HCID 642197—
反応物1-(10,11-Dihydro-5H-dibenzo[a,d]cyclohepten-5-yl)piperazineHCID 2735936—
反応物trans-7-(3-Chloroallyloxy)-2-methyl-benzothiazoleHCID 23289321—
生成物trans-7-{4-[4-(10,11-Dihydro-5H-dibenzo[a,d]cyclohepten-5-yl)-piperazin-1-yl]-but-2-enyloxy}-2-methyl-benzothiazoleHCID 23289240—
生成物trans-7-(3-Chloroallyloxy)-2-methyl-benzothiazoleHCID 23289321—

反応手順

The title compound was prepared according to Method GA from trans-7-(3-chloro-allyloxy)-2-methyl-benzothiazole and 1-(10,11-dihydro-5H-dibenzo[a,d]-cyclohepten-5-yl)piperazine. mp 151-152° C.; LSIMS m/z 496. The trans-7-(3-chloroallyloxy)-2-methyl-benzothiazole was prepared by Method IV with trans-1,4-dichloro-2-butene as the alkylating agent.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US06130217
出典データセットuspto-grants-2000_10
ORD IDord-0ee17759ccbc4c78b10e19e429ca0ccc
出典メモuspto-grants-2000_10