化工社化工社 化学情報印刷レポート · 研究参考用
Dehydrolinalool → Linalool
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Dehydrolinalool | HCID 62842 | — |
| 反応物 | HCID 178418361 | HCID 178418361 | — |
| 生成物 | Linalool | HCID 6549 | — |
反応手順
In a 300 ml pressure reactor, 10 g of the Ru catalyst as described in the catalyst production example were placed in a catalyst basket insert and 150 g (0.99 mol) of dehydrolinalool were added. The hydrogenation was carried out using pure hydrogen at a constant pressure of 40 bar and a temperature of 80° C. After a reaction time of 4 hours, the reactor was vented. The conversion of dehydrolinalool was 95% and linalool was obtained in a selectivity of 90%.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06130360 |
| 出典データセット | uspto-grants-2000_10 |
| ORD ID | ord-6e5a1006c86f40c6a0251bc3a7e52998 |
| 出典メモ | uspto-grants-2000_10 |