Benzoic Acid → 1,1,1,3,3,3-Hexafluoropropane
反応式
C(O)(=O)C1C=CC=CC=1.OC1C=CC([C:17](C2C=CC(O)=CC=2)([C:22]([F:25])([F:24])[F:23])[C:18]([F:21])([F:20])[F:19])=CC=1>>[F:19][C:18]([F:21])([F:20])[CH2:17][C:22]([F:25])([F:24])[F:23]参加物
3
実験手順
A reaction was conducted as described in Example 6 except that benzoic acid was replaced with 105 mmol of 2,2-bis(4-hydroxyphenyl)-1,1,1,3,3,3-hexafluoropropane and the amount of PGE was 200 mmol. Desired 2,2-bis[4-(2-hydroxy-3-phenoxypropyloxy)phenyl[-1,1,1,3,3,3-hexafluoropropane was formed in analytical yield of 89% and isolated in a yield of 83%.
出典と根拠
- ORDレコード
- ord-91ba050f309d4a999d59440f4a716774
- 出典データセット
- uspto-grants-2000_10
- 特許番号
- US06130346
反応ノート
読み込み中…