化工社化工社 化学情報印刷レポート · 研究参考用
Benzoic Acid → 1-(4-Chlorophenoxymethyl)-2-(2-methoxyethoxy)ethyl benzoate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Benzoic Acid | HCID 243 | — |
| 反応物 | 2-((4-Chlorophenoxy)methyl)oxirane | HCID 91515 | — |
| 反応物 | 2-Methoxyethyl benzoate | HCID 228741 | — |
| 溶媒 | 2-Methoxyethanol | HCID 8019 | — |
| 生成物 | 1-(4-Chlorophenoxymethyl)-2-(2-methoxyethoxy)ethyl benzoate | HCID 9950980 | 93% |
反応手順
A reaction was conducted as described in Example 6 except that benzoic acid was replaced with the same molar amount of 2-methoxyethyl benzoate, a compound represented by formula (3) where R2 is phenyl and OZ1 is an organic group derived from 2-methoxyethanol, and PGE was replaced with the same molar amount of 4-chlorophenyl glycidyl ether. Desired 1-(4-chlorophenoxymethyl)-2-(2-methoxyethoxy)ethyl benzoate was formed in an analytical yield of 93% and isolated in a yield of 86%.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06130346 |
| 出典データセット | uspto-grants-2000_10 |
| ORD ID | ord-ebe83e5750364f8bb5beeb9a960eb2ae |
| 出典メモ | uspto-grants-2000_10 |