化工社化工社 化学情報印刷レポート · 研究参考用
Ammonium thiocyanate → HCID 23287621、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ammonium thiocyanate | HCID 15666 | — |
| 反応物 | N-methylthiophen-3-amine | HCID 642344 | — |
| 反応物 | 2-Chloronicotinoyl chloride | HCID 2774541 | — |
| 溶媒 | Acetone | HCID 180 | — |
| 生成物 | HCID 23287621 | HCID 23287621 | 26.3% |
反応手順
The reaction procedure of Example 102 was followed except that 560 mg of 2-chloronicotinoyl chloride, 242 mg of ammonium thiocyanate, 360 mg of 3-(methylamino)thiophene and 10 ml of acetone were used. The product was then recrystallized from a mixture of ethanol and chloroform to obtain 230 mg of 2-[N-methyl-N-(3-thienyl)amino)-4H-pyrido[3,2-e]-1,3-thiazin-4-one.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06133258 |
| 出典データセット | uspto-grants-2000_10 |
| ORD ID | ord-f44349c4c9634de7b3e5f2bc8b5ad0da |
| 出典メモ | uspto-grants-2000_10 |