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Tris(pentafluorophenyl)borane → Tris(pentafluorophenyl)borane hydrate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Tris(pentafluorophenyl)borane | HCID 582056 | — |
| 反応物 | Borane, tris(pentafluorophenyl)-, trihydrate | HCID 11261567 | — |
| 溶媒 | Dichloromethane | HCID 6344 | — |
| 生成物 | Tris(pentafluorophenyl)borane hydrate | HCID 15875499 | — |
反応手順
A mixture of 0.566 gram (1 mmol) (C6F5)3B.3H2O as prepared in Example 1 and 1.024 grams (2 mmol) (C6F5)3B in 10 mL dichloromethane was stirred for 15 minutes and then evaporated to dryness under vacuum. A quantitative yield of the product remained and was stored under dry nitrogen.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05416177 |
| 出典データセット | uspto-grants-1995_05 |
| ORD ID | ord-947c77284e834395add5a41dba46ce12 |
| 出典メモ | uspto-grants-1995_05 |