1-Bromopentadecane → 2-(Heptadecyl)furan
反応式
[CH2:1]([C:16]1[O:17][CH:18]=[CH:19][CH:20]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH3:15].Br[CH2:22][CH2:23]CCCCCCCCCCCCC>>[CH2:1]([C:16]1[O:17][CH:18]=[CH:19][CH:20]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:22][CH3:23]参加物
3
実験手順
2-(heptadecyl)furan (4) was prepared exactly as described above for 2-(pentadecyl)furan, substituting 1-bromo heptadecane for 1-bromopentadecane. The chromatographed product was recrystallized from methanol as described above to afford of 2-(heptadecyl)furan (4) in 48% yield.
後処理
- custom2-(heptadecyl)furan (4) was prepared exactly
- customThe chromatographed product was recrystallized from methanol
出典と根拠
- ORDレコード
- ord-e98cdf64dc924ad89afde47098b4f488
- 出典データセット
- uspto-grants-2000_10
- 特許番号
- US06133313
反応ノート
読み込み中…