化工社化工社 化学情報印刷レポート · 研究参考用
Silane, chloro(chloromethyl)dimethyl- → n-Ethyl-2-chloro-6-[(chloromethyl)dimethylsilyl]benzamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Silane, chloro(chloromethyl)dimethyl- | HCID 74393 | — |
| 反応物 | 2-chloro-N-ethylbenzamide | HCID 347962 | — |
| 生成物 | n-Ethyl-2-chloro-6-[(chloromethyl)dimethylsilyl]benzamide | HCID 18630074 | — |
反応手順
The title compound was prepared from the compound of Example f and 2.0 eq (chloromethyl)dimethylsilyl chloride according to General Method C. Recrystallization from ethyl acetate gave 3.0 g of the desired compound as a white solid, a 52% yield. m.p. 88-89° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06133252 |
| 出典データセット | uspto-grants-2000_10 |
| ORD ID | ord-5559485b8ba34a3ba66d94109c8a8114 |
| 出典メモ | uspto-grants-2000_10 |