反応式
[F:1][C:2]1[C:10]2[S:9][C:8]([C:11](=O)[CH2:12][C:13](=O)[C:14]([F:17])([F:16])[F:15])=[N:7][C:6]=2[CH:5]=[CH:4][CH:3]=1.Cl.[S:21]([C:25]1[CH:30]=[CH:29][C:28]([NH:31][NH2:32])=[CH:27][CH:26]=1)(=[O:24])(=[O:23])[NH2:22]>>[F:1][C:2]1[C:10]2[S:9][C:8]([C:11]3[N:31]([C:28]4[CH:27]=[CH:26][C:25]([S:21]([NH2:22])(=[O:24])=[O:23])=[CH:30][CH:29]=4)[N:32]=[C:13]([C:14]([F:17])([F:16])[F:15])[CH:12]=3)=[N:7][C:6]=2[CH:5]=[CH:4][CH:3]=1参加物
3
実験手順
The procedure of Example 9 was repeated using 1-(7-fluorobenzothiazol-2-yl)-4,4,4-trifluorobutane-1,3-dione and 4-sulfamoylphenylhydrazine hydrochloride as the starting materials to obtain 4-[5-(7-fluorobenzothiazol-2-yl)-3-trifluoromethyl-1H-pyrazol-1-yl]benzenesulfonamide (yield, 88%).
出典と根拠
- ORDレコード
- ord-ee87f12a5e074065bc4d1fc3b61958c0
- 出典データセット
- uspto-grants-2000_10
- 特許番号
- US06136831
関連ノート
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