化工社化工社 化学情報印刷レポート · 研究参考用
Hydrochloric Acid → Acridine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydrochloric Acid | HCID 313 | — |
| 反応物 | Isatin | HCID 7054 | — |
| 溶媒 | Water | HCID 962 | — |
| 溶媒 | Potassium Hydroxide | HCID 14797 | — |
| 生成物 | Acridine | HCID 9215 | — |
反応手順
The isatin product was refluxed in 110 mL of 10% KOH solution in water over night. The dark green mixture was cooled and acidified with 400 mL of 1:1 ice/5M HCl. The solid was washed with water and air-dried yielding the acridine acid. 1H NMR (DMSO-d6) δ 7.81-7.94 (m, 4H), 8.31-8.36 (m, 2H).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06139782 |
| 出典データセット | uspto-grants-2000_10 |
| ORD ID | ord-5c84b6e6fadf4bc3a55ced04ab90b4ed |
| 出典メモ | uspto-grants-2000_10 |