化工社化工社 化学情報印刷レポート · 研究参考用
Chlorotrimethylsilane → Silane, trimethyl(trifluoroethenyl)-
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Chlorotrimethylsilane | HCID 6397 | — |
| 反応物 | Chlorotrifluoroethylene | HCID 6594 | — |
| 反応物 | Butyllithium | HCID 178418339 | — |
| 生成物 | Silane, trimethyl(trifluoroethenyl)- | HCID 11205884 | — |
反応手順
Chlorotrifluoroethylene of the formula (10) is treated with n-butyl lithium and then reacted with chlorotrimethylsilane of the formula (11) to obtain 1,1,2-trifluoro-2-trimethylsilylethylene of the formula (12). Then, without isolation, this compound (12) is reacted further with a lithium compound of the formula (13) to obtain a difluoroethylene compound of the formula (14).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05419851 |
| 出典データセット | uspto-grants-1995_05 |
| ORD ID | ord-d714a4907e85428cb8eae91d6d2f93c7 |
| 出典メモ | uspto-grants-1995_05 |