Hydroquinone → HCID 131714254、化合物

HRID 370423

反応式

HRID 370423 の反応式
[C:1]1([CH:8]=[CH:7][C:5]([OH:6])=[CH:4][CH:3]=1)[OH:2].[C:9](Cl)(=[O:27])[CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH:24]([CH3:26])[CH3:25]>>[C:9]([OH:27])(=[O:2])[CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH:24]([CH3:26])[CH3:25].[C:1]1([CH:8]=[CH:7][C:5]([OH:6])=[CH:4][CH:3]=1)[OH:2]

参加物

3

反応物 2

HCID 785HydroquinoneHCID 118402Heptadecanoyl chloride, 16-methyl-

生成物 1

HCID 131714254HCID 131714254、化合物

実験手順

According to the same procedure as described in Preparation 1, hydroquinone and isostearoyl chloride (prepared by chlorination of isostearic acid with thionyl chloride) were reacted and the reaction mixture was extracted with ethyl acetate. The extract was washed with water and the solvent was removed. The resulting residue was thoroughly washed with water to remove unreacted hydroquinone and concentrated on a water bath at 70° C. under the reduced pressure of 1 mmHg to give hydroquinone monoisostearate.

後処理

  1. customwere reacted
  2. extractionthe reaction mixture was extracted with ethyl acetate
  3. washThe extract was washed with water
  4. customthe solvent was removed
  5. washThe resulting residue was thoroughly washed with water
  6. customto remove unreacted hydroquinone
  7. concentrationconcentrated on a water bath at 70° C. under the reduced pressure of 1 mmHg

出典と根拠

ORDレコード
ord-e83c5b7767814b1191453355b65b50c0
出典データセット
uspto-grants-1985_07
特許番号
US04526779

関連ノート

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