化工社化工社 化学情報印刷レポート · 研究参考用
1,6-Hexanediol → 1,6-Bis(2,2,6,6-tetramethyl-4-piperidylamino)hexane
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1,6-Hexanediol | HCID 12374 | — |
| 反応物 | 4-Amino-2,2,6,6-tetramethylpiperidine | HCID 37524 | — |
| 反応物 | HCID 178418361 | HCID 178418361 | — |
| 生成物 | 1,6-Bis(2,2,6,6-tetramethyl-4-piperidylamino)hexane | HCID 93419 | — |
反応手順
A mixture of 4-amino-2,2,6,6-tetramethylpiperidine and 1,6-hexanediol in a molar ratio of 4:1 is reacted in a 1-liter shaft oven which is filled with 500 ml of reduced copper chromite catalyst (Harshaw Cu 1107 of Harshaw Chemical Co, DE-5632 Wermelskirchen) at 180° C. and 30 bars of hydrogen hourly.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04526971 |
| 出典データセット | uspto-grants-1985_07 |
| ORD ID | ord-87e7e1d3f09947258c8930b5f8efa942 |
| 出典メモ | uspto-grants-1985_07 |