化工社化工社 化学情報印刷レポート · 研究参考用
Atrazine → Atraton
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Atrazine | HCID 2256 | — |
| 反応物 | Cyprazine | HCID 24738 | — |
| 反応物 | Sodium Methoxide | HCID 10942334 | — |
| 反応物 | 2-Methoxy-4-(cyclopropylamino)-6-(1-methylethylamino)-1,3,5-triazine | HCID 20274862 | — |
| 溶媒 | Hexane | HCID 8058 | — |
| 生成物 | Atraton | HCID 15359 | — |
反応手順
2-methoxy-4-(1-methylethylamino)-6-ethylamino-1,3,5-triazine (14A) (Atraton) was prepared as a white solid (recrystallized from hexane), m.p.: 95°-96° C., by treating atrazine (Examples 5-8) with sodium methoxide according to the procedure described for preparing 13A from 9B, Example 13.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04528027 |
| 出典データセット | uspto-grants-1985_07 |
| ORD ID | ord-472066d724e641529f689e4d8224ee70 |
| 出典メモ | uspto-grants-1985_07 |