Hydrochloric Acid → Dodecylammonium chloride

HRID 371254ノート

反応式

HRID 371254 の反応式
[CH2:1]([NH2:13])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12].[ClH:14]>C(Cl)Cl>[ClH:14].[CH2:1]([NH2:13])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12]

参加物

4

反応物 2

HCID 313Hydrochloric AcidHCID 13583Dodecylamine

生成物 1

HCID 458426Dodecylammonium chloride収率 95.5%

試薬・触媒・溶媒 1

HCID 6344Dichloromethane溶媒

反応条件

温度
0 °C

実験手順

Dodecylamine (85 g, 0.46 mol) was dissolved in methylene chloride (500 mL). The solution was cooled to 0° C., and saturated with anhydrous hydrogen chloride (45 minutes). The white, crystalline solid was separated and dried in vacuum over phosphorus pentoxide, to provide 97.5 g (95.5%) of n-dodecylamine hydrochloride.

後処理

  1. customThe white, crystalline solid was separated
  2. dry with materialdried in vacuum over phosphorus pentoxide

出典と根拠

ORDレコード
ord-3610f441decb46118ba667e34d25705d
出典データセット
uspto-grants-1985_07
特許番号
US04530714

反応ノート

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