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3,4-Dichloroaniline → 2,2'-Dithiobis[N-(3,4-dichlorophenyl)benzamide]
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3,4-Dichloroaniline | HCID 7257 | — |
| 反応物 | 2,2'-Dithiodibenzoyl chloride | HCID 88164 | — |
| 溶媒 | Pyridine | HCID 1049 | — |
| 溶媒 | Dichloromethane | HCID 6344 | — |
| 生成物 | 2,2'-Dithiobis[N-(3,4-dichlorophenyl)benzamide] | HCID 18935342 | 10.2% |
反応手順
This compound was prepared according to the general method of Example 77 using 2,2'-dithiobisbenzoyl chloride (1.04 g, 3.03 mmol) in 25 mL of dichloromethane and 3,4-dichloroaniline (0.982 g, 6.06 mmol) in 8 mL of pyridine. The crude product was recrystallized from ethyl acetate-hexanes to yield 0.184 g of the title compound, mp 230°-233° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05734081 |
| 出典データセット | uspto-grants-1998_03 |
| ORD ID | ord-b17219fcebd74ae7ac99426fccd85e3c |
| 出典メモ | uspto-grants-1998_03 |