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HRID 371834作成日:2026年10月26日

19-Hydroxytestosterone → 1beta-Methyl-4-androstene-3alpha,17beta,19-triol

https://huagongshe.com/reaction/371834

反応式

関与物質

役割名称HCID仕込み量
反応物19-HydroxytestosteroneHCID 150968—
反応物19-Hydroxy-1beta-methyl-4-androsten-3,17-dioneHCID 54279369—
反応物17beta,19-Dihydroxy-7alpha-methyl-4-androsten-3-one diacetateHCID 86735689—
生成物1beta-Methyl-4-androstene-3alpha,17beta,19-triolHCID 70585106—

反応手順

Following essentially the same procedure and substituting 17β,19-dihydroxy-7α-methyl-4-androsten-3-one diacetate, 7α-methyl-17β,19-di-(2'-tetrahydropyranyloxy)-4-androsten-3-one and 19-hydroxy-1β-methyl-4-androsten-3,17-dione for the 17β,19-dihydroxy-4-androsten-3-one above results in the preparation of 7α-methyl-4-androstene-3α,17β,19-triol 17β,19-diacetate, 7α-methyl-17β,19-di-(2'-tetrahydropyranyloxy)-4-androsten-3α-ol and 1β-methyl-4-androstene-3α,17β,19-triol, respectively.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US04087524
出典データセットuspto-grants-1978_05
ORD IDord-b5685285bf2e498ea63e2e8449911c77
出典メモuspto-grants-1978_05