Methyl Acrylate → HCID 15919806、化合物

HRID 371894

反応式

HRID 371894 の反応式
[CH2:1]([NH2:17])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16].[C:18]([O:22][CH3:23])(=[O:21])[CH:19]=[CH2:20]>CO>[CH2:1]([NH:17][CH:19]([CH3:20])[C:18]([O:22][CH3:23])=[O:21])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16]

参加物

4

反応物 2

HCID 7294Methyl AcrylateHCID 8926Hexadecylamine

生成物 1

HCID 15919806HCID 15919806、化合物

試薬・触媒・溶媒 1

HCID 887Methanol溶媒

実験手順

66.4 g of hexadecylamine are dissolved in 250 ml of methanol. 27 ml of methyl acrylate are added and the mixture is left to stand overnight. After removal of the solvent by distillation the residue is recrystallised from ethyl acetate.

後処理

  1. waitthe mixture is left
  2. customAfter removal of the solvent
  3. distillationby distillation the residue
  4. customis recrystallised from ethyl acetate

出典と根拠

ORDレコード
ord-7c99f89006944ecc9fb1dc936a498189
出典データセット
uspto-grants-1978_05
特許番号
US04088491

関連ノート

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