Methyl Acrylate → Methyl 2-hexadecylaminopropionate
反応式
[CH2:1]([NH2:17])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16].[C:18]([O:22][CH3:23])(=[O:21])[CH:19]=[CH2:20]>CO>[CH2:1]([NH:17][CH:19]([CH3:20])[C:18]([O:22][CH3:23])=[O:21])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16]参加物
4
実験手順
66.4 g of hexadecylamine are dissolved in 250 ml of methanol. 27 ml of methyl acrylate are added and the mixture is left to stand overnight. After removal of the solvent by distillation the residue is recrystallised from ethyl acetate.
後処理
- waitthe mixture is left
- customAfter removal of the solvent
- distillationby distillation the residue
- customis recrystallised from ethyl acetate
出典と根拠
- ORDレコード
- ord-7c99f89006944ecc9fb1dc936a498189
- 出典データセット
- uspto-grants-1978_05
- 特許番号
- US04088491
反応ノート
読み込み中…