化工社化工社 化学情報印刷レポート · 研究参考用
Butylamine → HCID 178449232、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Butylamine | HCID 8007 | — |
| 反応物 | Methyl hydrazinecarbimidothioate hydroiodide | HCID 6508896 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | HCID 178449232 | HCID 178449232 | — |
反応手順
S-Methylisothiosemicarbazide hydroiodide (46.6 g) and 1-aminobutane (48 ml) and water (100 ml) were heated under reflux for 1 hour. The resulting solution was evaporated to an oil which was crystallised from amyl alcohol/80-100 PE, to give the title compound (a).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04089962 |
| 出典データセット | uspto-grants-1978_05 |
| ORD ID | ord-f2bacff0b3604575b7f45e3420a48d67 |
| 出典メモ | uspto-grants-1978_05 |