Methylcarbamyl fluoride → N-Methyl-N(t-Octylthiosulfenyl)Carbamoyl Fluoride

反応式

[C:1]([S:9][S:10]Cl)([CH2:4][C:5]([CH3:8])([CH3:7])[CH3:6])([CH3:3])[CH3:2].[CH3:12][NH:13][C:14]([F:16])=[O:15]>>[CH3:12][N:13]([S:10][S:9][C:1]([CH2:4][C:5]([CH3:8])([CH3:7])[CH3:6])([CH3:3])[CH3:2])[C:14]([F:16])=[O:15]

参加物

反応物 2

HCID 12545956Methylcarbamyl fluoride

HCID 85958550t-Octylthiosulfenylchloride

生成物 1

HCID 85958536N-Methyl-N(t-Octylthiosulfenyl)Carbamoyl Fluoride

実験手順

Prepared by the procedure of Example II by reacting t-octylthiosulfenylchloride with methylcarbamoyl fluoride. b.p. 112° C/0.5 Torr ND23 1.4960.

後処理

customPrepared by the procedure of Example II

出典と根拠

ORDレコード: ord-abaf12c3350b4f309bd150afc0b462f1
出典データセット: uspto-grants-1978_05
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US04091016

反応ノート

読み込み中…