Methylcarbamyl fluoride → N-Methyl-N(Phenylthiosulfenyl)Carbamoyl Fluoride

反応式

[C:1]1([S:7][S:8]Cl)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH3:10][NH:11][C:12]([F:14])=[O:13]>>[CH3:10][N:11]([S:8][S:7][C:1]1[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1)[C:12]([F:14])=[O:13]

参加物

反応物 2

HCID 12545956Methylcarbamyl fluoride

HCID 15683250Phenylthiosulfenyl chloride

生成物 1

HCID 23332999N-Methyl-N(Phenylthiosulfenyl)Carbamoyl Fluoride

実験手順

Prepared by the procedure of Example II by reacting phenylthiosulfenyl chloride with methylcarbamoyl fluoride. b.p. 100°-110° C/0.3 Torr ND22.5 1.5770.

後処理

customPrepared by the procedure of Example II

出典と根拠

ORDレコード: ord-a948376d85b24205a633fefe4353694e
出典データセット: uspto-grants-1978_05
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US04091016

反応ノート

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