Methylcarbamyl fluoride → N-Methyl-N(4-Methylphenylthiosulfenyl)Carbamoyl Fluoride

反応式

[CH3:1][C:2]1[CH:7]=[CH:6][C:5]([S:8][S:9]Cl)=[CH:4][CH:3]=1.[CH3:11][NH:12][C:13]([F:15])=[O:14]>>[CH3:11][N:12]([S:9][S:8][C:5]1[CH:6]=[CH:7][C:2]([CH3:1])=[CH:3][CH:4]=1)[C:13]([F:15])=[O:14]

参加物

反応物 2

HCID 12545956Methylcarbamyl fluoride

HCID 204720224-Methylphenylthiosulfenyl chloride

生成物 1

HCID 23332987N-Methyl-N(4-Methylphenylthiosulfenyl)Carbamoyl Fluoride

実験手順

Prepared by the procedure of Example II by reacting 4-methylphenylthiosulfenyl chloride with methylcarbamoyl fluoride. b.p. 92°-100° C/0.25 Torr ND22.5 1.5735.

後処理

customPrepared by the procedure of Example II

出典と根拠

ORDレコード: ord-7b41765762ab4fd295037eca88a267ca
出典データセット: uspto-grants-1978_05
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US04091016

反応ノート

読み込み中…