Methylcarbamyl fluoride → N-methyl-N-(4-chlorophenylthiosulfenyl)carbamoyl fluoride

反応式

[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([S:8][S:9]Cl)=[CH:4][CH:3]=1.[CH3:11][NH:12][C:13]([F:15])=[O:14]>>[CH3:11][N:12]([S:9][S:8][C:5]1[CH:6]=[CH:7][C:2]([Cl:1])=[CH:3][CH:4]=1)[C:13]([F:15])=[O:14]

参加物

反応物 2

HCID 12545956Methylcarbamyl fluoride

HCID 134417494-Chlorophenylthiosulfenyl chloride

生成物 1

HCID 23333002N-methyl-N-(4-chlorophenylthiosulfenyl)carbamoyl fluoride

実験手順

Prepared by the procedure of Example II by reacting 4-chlorophenylthiosulfenyl chloride with methylcarbamoyl fluoride. b.p. 110°-113° C/0.3 Torr ND24 1.5959.

後処理

customPrepared by the procedure of Example II

出典と根拠

ORDレコード: ord-5190e15b808e43d98e4be39d36ec4870
出典データセット: uspto-grants-1978_05
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US04091016

反応ノート

読み込み中…